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Chemical Overview


Iraq established a Chemical Corps in the mid-1960s, tasked with the nuclear, biological and chemical protection of troops and civilians. The Corps developed a laboratory-scale facility in the early 1970s to gain practical experience in synthesizing chemical warfare (CW) agents and evaluating their properties. The laboratory's work constituted a necessary step in the training of a national cadre for future research and production of offensive chemical weapons. In addition, it contributed to the creation of a support infrastructure and acquisition system for equipment and materials.[1]

Iraq invaded Iran in 1980 and, following a series of military defeats in 1981 and 1982, Iraq began to employ chemical weapons against Iranian forces. In 1988, in the closing stages of the war, Iraq mounted a massive chemical attack against the Kurdish town of Halabja, killing approximately 5,000 civilians.

Iraq's capacity to develop chemical weapons was greatly assisted by its ability to import precursor chemicals and production equipment, and obtain technical support from Western suppliers.[2] Iraq eventually produced mustard blister agent and nerve agents such as tabun, sarin, and VX. Following its defeat by the United States and allied forces in 1991, Iraq declared to UN inspectors that between 1982 and 1990 it produced 3,859 tons of CW agents and more than 125,000 filled and unfilled special munitions, most of which was stored at the Muthanna State Establishment, Iraq's primary CW production, filling, and testing facility. This declaration served as the basis for United Nations Special Commission (UNSCOM) inspectors' subsequent efforts to verify the destruction of all Iraqi CW agents.

By December 1998, UNSCOM inspectors had destroyed 38,537 filled and unfilled chemical munitions, 690 metric tons of CW agents, more than 3,275 metric tons of precursor chemicals, over 425 pieces of key production equipment, and 125 pieces of analytical instruments.[3] Taking into account items unilaterally destroyed by Iraq prior to the beginning of inspections, UNSCOM was able to account for the destruction of 88,000 filled and unfilled chemical munitions, over 690 metric tons of weaponized and bulk CW agents, approximately 4,000 metric tons of precursor chemicals, 980 pieces of key production equipment, and 300 pieces of analytical instruments.[4]

UNSCOM's final report to the UN Security Council noted a number of outstanding issues arising from efforts to verify the accuracy of Iraq's declarations. These included discrepancies regarding Iraq's use of chemical weapons during the 1980s resulting in UNSCOM being unable to satisfactorily account for 550 artillery shells filled with mustard agent declared to have been lost shortly after the Gulf War and approximately 500 R-400 aerial bombs. UNSCOM was also concerned over a lack of information regarding Iraq's production of VX agent and its plans for the use the agent, and inadequate accounting of the disposition of precursors used in the production of VX agent.[5]

In August 1998, Iraq unilaterally declared that all outstanding CW-related disarmament issues had been resolved and effectively ceased to cooperate with UNSCOM. This ultimately led to UNSCOM's withdrawal in December 1998 followed by Operation Desert Fox, in which the United States and Great Britain bombed a number of facilities thought to be associated with reviving Iraq's WMD programs.

International sanctions against Iraq were maintained in the continuing belief that it was secretly storing a significant quantity of CW agent, particularly nerve agent, and was in a position to rebuild much of its chemical weapons production infrastructure.

From January 1999 to November 2002, very little new information became available regarding Iraqi attempts to revive WMD programs. However, given Iraq's past efforts to conceal its activities and retain its capabilities, Western intelligence agencies considered it likely that UNSCOM's withdrawal had led to a restoration of CW production capabilities. Intelligence provided by Iraqi opposition groups such as the Iraqi National Congress (INC) reinforced these concerns.

In November 2002, following a period of escalating pressure on Iraq, the United Nations Monitoring, Verification and Inspection Commission (UNMOVIC) inspection teams (successors to UNSCOM inspectors) were finally allowed access to Iraq. Between November 27, 2002 and March 18, 2003, UNMOVIC conducted 731 inspections covering 411 sites, 88 of which had not been inspected previously.[6] In addition, UNMOVIC was able to conduct 14 interviews with Iraqi personnel. On March 18, 2003, UNMOVIC inspection efforts ended with the withdrawal of all personnel from Iraq in anticipation of U.S.-led military action.

The UNMOVIC inspections were able to verify the destruction of between 30 and 39 per cent of Iraq's declared stockpile of 1.5 metric tons of VX. They also identified a small number of CW munitions that appeared to have been produced prior to 1990. UNMOVIC concluded that it had not found evidence of the continuation or resumption of WMD programs.[7]

The U.S. government refused to accept the validity of UNMOVIC's conclusions and continued to assert that Iraq had failed to account for 1.5 tons of VX, 1,000 tons of mustard gas, and 550 munitions containing mustard gas. Thus, the United States accused Iraq of violating UN Security Council Resolution 1441 that required Iraq to cooperate with UN inspections.

On March 19, 2003, a U.S.-led coalition invaded Iraq and following the defeat of Iraq's armed forces overthrew Saddam Hussein's regime. One justification for military action was the suspicion that Iraq had clandestinely amassed large stockpiles of chemical weapons including VX, sarin and mustard gas, among other WMD that it had successfully concealed from the United Nations.

Following the overthrow of Saddam Hussein in April 2003, the United States tasked the Iraq Survey Group (ISG), headed by former UN inspector David Kay, with locating suspected WMD stockpiles and equipment. The process of searching for evidence of Iraqi WMD programs was greatly complicated by the country's large size; an ongoing insurgency that made unescorted travel extremely dangerous, and the destruction of most official Iraqi government archives in the closing stages of the 2003 war. In January 2004, David Kay resigned as head of the ISG and began to criticize the underlying premises of the group's work. On the basis of his work with the ISG, Kay rejected suggestions that there had been any significant Iraqi WMD activities since the end of the first Gulf War. Dr. Kay was replaced as head of the ISG by former UNSCOM member Charles A. Duelfer.

On September 30, 2004, the ISG released its final report on Iraq's WMD programs. Its key findings regarding Iraqi chemical weapons programs were as follows:

  • Saddam never abandoned his intentions to resume a CW effort when sanctions were lifted and conditions were judged favorable.
  • While a small number of old, abandoned chemical munitions have been discovered, ISG judges that Iraq unilaterally destroyed its undeclared chemical weapons stockpile in 1991.
  • Iraq's CW program was crippled by the Gulf War and the legitimate chemical industry, which suffered under sanctions, only began to recover in the mid-1990s. Subsequent changes in the management of key military and civilian organizations, followed by an influx of funding and resources, provided Iraq with the ability to reinvigorate its industrial base.
  • The way Iraq organized its chemical industry after the mid-1990s allowed it to conserve the knowledge-base needed to restart a CW program, conduct a modest amount of dual-use research, and partially recover from the decline of its production capability caused by the effects of the Gulf War and UN-sponsored destruction and sanctions.
  • Iraq constructed a number of new plants starting in the mid-1990s that enhanced its chemical infrastructure, although its overall industry had not fully recovered from the effects of sanctions, and had not regained pre-1991 technical sophistication or production capabilities prior to Operation Iraqi Freedom (OIF).
  • ISG uncovered information that the Iraqi Intelligence Service (IIS) maintained throughout 1991 to 2003 a set of undeclared covert laboratories to research and test various chemicals and poisons, primarily for intelligence operations.
  • ISG investigated a series of key pre-OIF indicators involving the possible movement and storage of chemical weapons, focusing on 11 major depots assessed to have possible links to CW. A review of documents, interviews, available reporting, and site exploitations revealed alternate, plausible explanations for activities noted prior to OIF which, at the time, were believed to be CW-related.[8]

Over the course of the period April 2003 to December 2004, a series of events highlighted the lack of security for sites formerly associated with Iraqi WMD programs. These events included the looting of IAEA sealed facilities at the Baghdad Nuclear Research Center (Tuwaitha) and the discovery of missile parts with UNMOVIC tags still attached in European scrap yards. The ISG noted that all the sealed buildings at the Muthanna State Establishment containing various items associated with the Iraqi chemical weapons program had been breached and some equipment and materials removed. These buildings had been inspected and sealed by UNSCOM/UNMOVIC inspectors and contained various items including chemical processing equipment that had been destroyed or rendered harmless, empty 155 millimeter artillery shells, and sarin filled rockets dating back to the 1980s.[9] It is unclear how much of this material was removed but it is unlikely to be useful for CW purposes.

Following the conclusion of the primary phase of the U.S. military operations in the city of Fallujah, the U.S. Marine Corps released photographs documenting what it described as a "chemical / explosives weapons laboratory." It was claimed that this laboratory which was clearly being used for the production of improvised explosive devices (IEDs) "may have served as a testing and research area for construction of improvised chemical devices (ICDs)."[10] Currently there are no indications that insurgents had actually produced chemical weapons at this or any other facility in Fallujah.

The ongoing insurgency in Iraq has included several attempts to produce chemical weapons or alternatively use industrial chemicals as weapons. In late 2003, an Iraqi insurgent group that maintained ties to Abu Musab al- Zarqawi, the "al-Abud network" managed to secure the services of an Iraqi chemist with a view to manufacturing Tabun nerve agent (GA) and nitrogen mustard (HN).[11] The group's efforts to produce CW agents were completely ineffective due to a combination of inadequate skills and difficulties securing suitable precursors. An effort by another Iraqi group to produce hydrogen cyanide for incorporation into IEDs also failed and was discovered in November 2004.[12] Even if successful this latter effort would not have produced a useful weapon given hydrogen cyanide's flammable nature and the problems with achieving lethal concentrations in the open-air.

In late 2006 and early 2007, insurgents launched a series of attacks, primarily in the Baghdad area, using canisters of chlorine stolen from water-processing facilities.[13] Although these attacks were initially ineffective, by the end of the cycle the attacks were beginning to produce casualties. In the most destructive attack on March 16, 2007, at least 250 people were injured after exposure to a chlorine gas cloud. Although a small number of victims were hospitalized, no deaths were caused by the released gas. Chlorine gas attacks ended shortly afterwards, but security forces continued to discover chlorine gas canisters in insurgent arms caches as late as early 2008.

Treaty Status

Iraq acceded to the Geneva Protocol banning the first use of chemical weapons in September 1931. In November 2007, Iraq completed the domestic legislative requirements for accession to the Chemical Weapons Convention (CWC). On January 13, 2009, Iraq submitted its accession document to the United Nations and became the 186th CWC member nation on February 12, 2009.[14] Iraq has formed a National Monitoring Directorate to implement the country's obligations under the CWC. On March 12, 2009, Iraq submitted its initial declaration to the Organisation for the Prohibition of Chemical Weapons (OPCW), "declaring two bunkers with filled and unfilled chemical weapons munitions, some precursors, as well as five former chemical weapons production facilities (CWPFs)."[15] The OPCW must conduct inspections to verify the accuracy of Iraq's initial CW declaration but as of July 2009 had not yet done so.[16] In addition Iraq should have submitted a plan for the destruction of the remaining chemical weapons listed in its initial declaration to the OPCW Executive Council for review and approval no later than March 14, 2009 which it appears to have done.[17] The Director-General of the OPCW noted that Iraq had submitted "additional information on the general plans for destruction of its chemical weapons and former production facilities" on April 20, 2009.[18]

Sources:
[1] For a more detailed discussion of the development and operation of Iraq's CW capability see"The Chemical Weapons Programme" in Compendium of Iraq's Proscribed Weapons Programmes in the Chemical, Biological and Missile Areas (New York, NY: United Nations, 2007) pp. 49-76, www.un.org/ Depts/ unmovic/ new/ documents/ compendium/ Chapter_III.pdf
[2] Jonathan B. Tucker, Trafficking Networks for Chemical Weapons Precursors: Lessons from the Iran-Iraq War of the 1980s (Monterey, CA: Monterey Institute of International Studies, 2008), cns.miis.edu/ opapers/ pdfs/ op13_tucker.pdf
[3] Thirteenth quarterly report on the activities of the United Nations Monitoring, Verification and Inspection Commission in accordance with paragraph 12 of Security Council resolution 1284, S/2003/580, May 30, 2003, United Nations Security Council, p. 40, www.un.org/ Depts/ unmovic/ new/ documents/ quarterly_ reports/ s-2003 -580.pdf.
[4] The "Amorim report," UN Security Council Document S/1999/356, Annex 1 para. 19.
[5] Ibid., para. 21.
[6] Thirteenth quarterly report on the activities of the United Nations Monitoring, Verification and Inspection Commission in accordance with paragraph 12 of Security Council resolution 1284, S/2003/580, May 30, 2003, United Nations Security Council, p. 6, www.un.org/ Depts/ unmovic/ new/ documents/ quarterly_ reports/ s-2003- 580.pdf
[7] Ibid., p. 5.
[8] Comprehensive Report of the Special Advisor to the DCI on Iraq's WMD Volume 3, (Washington, DC: GPO, September 2004), pp. 1-3,www.foia.cia.gov/ duelfer/ Iraqs_WMD_ Vol3.pdf
[9] Nineteenth quarterly report on the activities of the United Nations Monitoring, Verification and Inspection Commission in accordance with paragraph 12 of Security Council resolution 1284, S/2004/924, November 26, 2004, United Nations Security Council, p. 3 and 5, www.un.org/ Depts/ unmovic/ new/ documents/ quarterly_ reports/ s-2004- 924.pdf
[10] Fallujah Update, Insurgent Chemical/Explosives Weapons Laboratory, Multi-National Force, November 26, 2004, www.globalsecurity.org/ wmd/ library/ report/ 2004/ fallujah-cw_ cpic_26nov2004.ppt.
[11] Comprehensive Report of the Special Advisor to the DCI on Iraq's WMD Volume 3, Annex E (Washington, DC: GPO, September 2004), pp. 93-94, www.foia.cia.gov/ duelfer/ Iraqs_ WMD_Vol3.pdf
[12] Bill Gertz, "Iraqi bomb labs signal attacks in the works," The Washington Times, November 30, 2004, www.washingtontimes.com/ news/ 2004/ nov/ 30/ 20041130- 121437- 7453r/ print/
[13] Richard Weitz, Ibrahim Al-Marashi and Khalid Hilal, "Chlorine as a Terrorist Weapon in Iraq," WMD Insights, Issue 15, May 2007, pp. 9-16, www.wmdinsights.com/ I15/ I15_ ME1_ Chlorine.htm
[14] Iraq Joins the Chemical Weapons Convention, Organisation for the Prohibition of ChemicalWeapons, January 14, 2009, www.opcw.org/ news/ news/ article/ iraq- joins- the- chemical- weapons- convention/.
[15] Opening Statement by the Director General to the Executive Council at its Fifty-Sixth Session, EC-56/DG.10, p. 2, www.opcw.org/ index.php? eID= dam_ frontend_ download& fileID=12961.
[16] Opening Statement by the Director General to the Executive Council at its Fifty-Seventh Session, EC-57/DG.15, Organisation for the Prohibition of Chemical Weapons, July 14, 2009, www.opcw.org/ index.php? eID= dam_ frontend_ download& fileID=13263. Part III(A) of the CWC Verification Annex does not specify timing for the initial inspection beyond requiring that it be conducted "promptly."
[17] Article III, paragraph 1 (a) (v) of the CWC requires that a member state provide its general plan for destruction of chemical weapons that it owns or possesses, or that are located in any place under its jurisdiction or control not later than 30 days after the Convention enters into force for it. www.opcw.org/ chemical- weapons- convention/ articles/ article- iii- declarations/
[18] Opening Statement by the Director General to the Executive Council at its Fifty-Sixth Session, EC-56/DG.10, p. 2, www.opcw.org/ index.php? eID= dam_ frontend_ download& fileID=12961.

 

Updated September 2009



Iraq Maps
The Biological Weapons Convention (BWC)
Addressing the Spread of Cruise Missiles and Unmanned Air Vehicles (UAVs)
To Comply or Not to Comply: Outline of the UN Inspections Mechanism in Iraq
WMD in the Middle East
Dusty Agents and the Iraqi Chemical Weapons Arsenal
U.S. and Hostile Powers: Iraq
Limiting the Use of WMD between Regional Powers: Iran vs. Iraq—Options
Treaties and Organizations
Senate Intel Panel Releases Two Iraq Reports (2006)
In Focus: IAEA and Iraq (2005)
UNMOVIC 21st Quarterly Report (2005),
Comprehensive Report of the Special Advisor to the DCI on Iraq’s WMD (2004)
Saddam's Iraq and Weapons of Mass Destruction: Iraq as a Case Study of a Middle Eastern Proliferant (2004)
Duelfer Report (BW & CW sections) [70 Mb] (2004)
18th quarterly report of UNMOVIC to the UN Sec General from 27 Aug 2004
17th quarterly report of UNMOVIC to the UN Sec General from 28 May 2004
Redirection of WMD Scientists in Iraq and Libya (2004)
16th quarterly report of UNMOVIC to the UN Sec General from 27 Feb 2004
WMD in Iraq: Evidence and Implications (2004)
The War in Iraq: An Intelligence Failure? (2003)
Disarming Iraq by Force: WMD Stakes and Scenarios (2003)
Iraq: Weapons of Mass Destruction (WMD) Capable Missiles and Unmanned Aerial Vehicles (UAVs) (2003)
International Atomic Energy Agency: Iraq Action Team (2003)
Unresolved Disarmament Issues: Iraq's Proscribed Weapons Programmes (2003)
Iraq's Weapons of Mass Destruction: A Net Assessment (2002)
Federation of American Scientists: Iraq Missile Guide (2000)
The Future of Chemical and Biological Disarmament in Iraq: From UNSCOM to UNMOVIC (1999)
UNSCOM's Comprehensive Review
Strengthening the BWC: Lessons from the UNSCOM Experience (1997)
Monitoring and Verification in a Noncooperative Environment: Lessons from the UN Experience in Iraq (1996)
Bill of Indictment: German Court Case Involving Iraq's Weapon Procurement (1993)
Iraq's Chemical and Biological Capability in the Kuwait Theater of Operations (1990)



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CNSThis material is produced independently for NTI by the James Martin Center for Nonproliferation Studies at the Monterey Institute of International Studies and does not necessarily reflect the opinions of and has not been independently verified by NTI or its directors, officers, employees, agents. Copyright © 2009 by MIIS.

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